Monitoring the staling of wheat bread using 2D MIR-NIR correlation spectroscopy
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Monitoring the staling of wheat bread using 2D MIR-NIR correlation spectroscopy. / Ringsted, Tine; Siesler, Heinz Wilhelm; Engelsen, Søren Balling.
I: Journal of Cereal Science, Bind 75, 2017, s. 92-99.Publikation: Bidrag til tidsskrift › Tidsskriftartikel › Forskning › fagfællebedømt
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TY - JOUR
T1 - Monitoring the staling of wheat bread using 2D MIR-NIR correlation spectroscopy
AU - Ringsted, Tine
AU - Siesler, Heinz Wilhelm
AU - Engelsen, Søren Balling
PY - 2017
Y1 - 2017
N2 - Staling of bread is a major source of food waste and efficient monitoring of it can help the food industry in the development of anti-staling recipes. While the staling fingerprint in the mid-infrared region is fairly well established this paper set out to find the most informative parts of the near-infrared spectra with respect to staling. For this purpose, two-dimensional correlation spectroscopy on near- and mid-infrared spectra of wheat bread crumb during aging was employed for the first time. The important mid-infrared absorption band at 1047 cm−1 related to amylopectin retrogradation was found to correlate positively with increased bread hardness and to co-vary with the near-infrared band at 910 nm in the short wavelength region (r2 = 0.88 to hardness), the near-infrared band at 1688 nm in the 1. overtone region (r2 = 0.97 to hardness) and to the near-infrared band in the long wavelength region at 2288 nm (r2 = 0.97 to hardness). The spectral information from the first principal component on near-infrared and the first principal component on mid-infrared was found to be highly correlated by a r2 = 0.98. It is demonstrated that the major bread staling processes such as amylopectin retrogradation and water loss can be followed with both near- and mid-infrared spectroscopy.
AB - Staling of bread is a major source of food waste and efficient monitoring of it can help the food industry in the development of anti-staling recipes. While the staling fingerprint in the mid-infrared region is fairly well established this paper set out to find the most informative parts of the near-infrared spectra with respect to staling. For this purpose, two-dimensional correlation spectroscopy on near- and mid-infrared spectra of wheat bread crumb during aging was employed for the first time. The important mid-infrared absorption band at 1047 cm−1 related to amylopectin retrogradation was found to correlate positively with increased bread hardness and to co-vary with the near-infrared band at 910 nm in the short wavelength region (r2 = 0.88 to hardness), the near-infrared band at 1688 nm in the 1. overtone region (r2 = 0.97 to hardness) and to the near-infrared band in the long wavelength region at 2288 nm (r2 = 0.97 to hardness). The spectral information from the first principal component on near-infrared and the first principal component on mid-infrared was found to be highly correlated by a r2 = 0.98. It is demonstrated that the major bread staling processes such as amylopectin retrogradation and water loss can be followed with both near- and mid-infrared spectroscopy.
KW - 2DCOS
KW - Bread staling
KW - Mid-infrared spectroscopy
KW - Near-infrared spectroscopy
U2 - 10.1016/j.jcs.2017.03.006
DO - 10.1016/j.jcs.2017.03.006
M3 - Journal article
AN - SCOPUS:85016564955
VL - 75
SP - 92
EP - 99
JO - Journal of Cereal Science
JF - Journal of Cereal Science
SN - 0733-5210
ER -
ID: 176653491