Chemical and physical characterization of Konjac glucomannan-based powders by FTIR and 13C MAS NMR
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Chemical and physical characterization of Konjac glucomannan-based powders by FTIR and 13C MAS NMR. / Da Silva, Denise Felix; Ogawa, Camilla Yara Langer; Sato, Francielle; Neto, Antonio Medina; Larsen, Flemming Hofmann; Matumoto-Pintro, Paula Toshimi.
In: Powder Technology, Vol. 361, 2020, p. 610-616.Research output: Contribution to journal › Journal article › Research › peer-review
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TY - JOUR
T1 - Chemical and physical characterization of Konjac glucomannan-based powders by FTIR and 13C MAS NMR
AU - Da Silva, Denise Felix
AU - Ogawa, Camilla Yara Langer
AU - Sato, Francielle
AU - Neto, Antonio Medina
AU - Larsen, Flemming Hofmann
AU - Matumoto-Pintro, Paula Toshimi
PY - 2020
Y1 - 2020
N2 - Konjac glucomannan (KGM) is extracted from Amorphophallus konjac tuber and composed of β-1,4 linked D-mannose and D-glucose. We aimed to produce and characterize KGM-based powders manufactured from dried (55°C-KF55 and 75°C-KF75) konjac tubers and compare to a commercial konjac glucomannan (CKG) powder. Structural characteristics on molecular, compositional, and microstructure levels as well as rehydration properties were assessed. Both compositional analysis as well as FTIR and 13C MAS NMR spectral analysis demonstrated a higher amount of protein than KF55 sample. The ratio between the two monomer units (D-mannose and D-glucose) was 1.6:1 in KF75, whereas it was 1.4:1 and 1.2:1 for KF55 and CKG, respectively, indicating slightly higher Man:Glc ratios in the KF samples. Decreased rehydration properties and flow index behavior (in solution) were observed in the konjac flours. Thus, differences were significant; konjac flours also presented good functionality, thereby, a good alternative to be used as hydrocolloid in food formulations.
AB - Konjac glucomannan (KGM) is extracted from Amorphophallus konjac tuber and composed of β-1,4 linked D-mannose and D-glucose. We aimed to produce and characterize KGM-based powders manufactured from dried (55°C-KF55 and 75°C-KF75) konjac tubers and compare to a commercial konjac glucomannan (CKG) powder. Structural characteristics on molecular, compositional, and microstructure levels as well as rehydration properties were assessed. Both compositional analysis as well as FTIR and 13C MAS NMR spectral analysis demonstrated a higher amount of protein than KF55 sample. The ratio between the two monomer units (D-mannose and D-glucose) was 1.6:1 in KF75, whereas it was 1.4:1 and 1.2:1 for KF55 and CKG, respectively, indicating slightly higher Man:Glc ratios in the KF samples. Decreased rehydration properties and flow index behavior (in solution) were observed in the konjac flours. Thus, differences were significant; konjac flours also presented good functionality, thereby, a good alternative to be used as hydrocolloid in food formulations.
KW - Amorphophallus konjac
KW - FTIR
KW - Glucomannan
KW - Konjac flour
KW - NMR
U2 - 10.1016/j.powtec.2019.11.071
DO - 10.1016/j.powtec.2019.11.071
M3 - Journal article
AN - SCOPUS:85075875226
VL - 361
SP - 610
EP - 616
JO - Powder Technology
JF - Powder Technology
SN - 0032-5910
ER -
ID: 235853216